WebDec 15, 2024 · Section snippets Preparation of Ni 3 (HITP) 2. Ni 3 (2,3,6,7,10,11-hexaaminotriphenelene) 2 was prepared by mixing 2,3,6,7,10,11-hexaaminotriphenylene hexahydrochloride (HATP.6HCl) to nickel chloride hexahydrate (NiCl 2.6H 2 O) following the procedure given by Sheberla and co-workers [35]. Briefly, 201.2 mg of HATP.6HCl … WebFeb 18, 2024 · In 2014, Dincă et al. developed a systematic method for producing an HATP·6HCl-based 2D MOF with good crystallinity and high electrical conductivity . Sophisticated characterization methods were applied to determinate the crystalline structure of Ni 3 (HITP) 2 .
2,3,6,7,10,11-六氨基三苯六盐酸盐 CAS#: 1350518-27-2
WebFeb 5, 2024 · NiCl 2.6H 2 O aqueous solution (0.01 mmol), NH 3 ·H 2 O (0.5 mL), and HATP·6HCl aqueous solution (0.01 mmol) were mixed at 25.0 °C under strong stirring for 30 min. After that, the prepared solution was transferred into Teflon autoclave at 100 °C during 5 h. After cooling treatment at 25.0 °C, the centrifugation treatment provided a green ... WebMay 25, 2024 · is added dr opwise to a s olution of 18.4 m g HATP·6HCl (0.033 mmol) dissolved in 5 mL me thanol upon stirring. The mixture is th en . added dropwise to a solution mixture of 77 mg ... kate winslet little children red bathing suit
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WebAbstract. Reaction of 2,3,6,7,10,11-hexaaminotriphenylene hexahydrochloride (HATP·6HCl) and (Tp Ph Ni)Cl (Tp Ph = tris(3,5-diphenyl-1-pyrazolyl)borate) produces the radical-bridged trinickel complex [(Tp Ph Ni) 3 (HITP)] (HITP 3− ˙ = 2,3,6,7,10,11-hexaiminotriphenylene). Magnetic measurements and broken-symmetry density functional theory calculations … WebHATP·6HCl was treated with an aqueous solution of NiCl 2· 6H 2 O under air, followed by the addition of aqueous NH 3 under constant stirring. The reaction mixture was heated to 65 °C and stirred under air for an additional 2 h. This yielded the new material Ni 3 (HITP) 2 (HITP = 2,3,6,7,10,11-hexa-iminotriphenylenesemiquinonate) as a bulk ... Webhexahydrochloride (HATP 6HCl) with ammoniacal NiCl2 produces a new crystalline s-MOG with very high electrical conductivity, which is linearly proportional to temperature. … kate winslet little children in laundry room